Shanxian Chemical
Products

Tetrabutylphonium Hydroxide

Shanxian Chemical

Specifications

HS Code

322141

Packing & Storage
Packing 100 - gram bottle of Tetrabutylphosphonium Hydroxide, securely sealed for chemical storage.
Storage Tetrabutylphosphonium Hydroxide should be stored in a cool, dry, well - ventilated area, away from heat sources and open flames. It is highly reactive, so keep it separated from oxidizing agents, acids, and other incompatible substances. Store in tightly sealed containers to prevent moisture absorption and evaporation, as it can degrade upon exposure to air and moisture.
Shipping Tetrabutylphosphonium Hydroxide is shipped in containers designed to prevent leakage. Due to its chemical nature, it's handled with care, ensuring compliance with hazardous material shipping regulations during transit.
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General Information
Frequently Asked Questions
What are the main uses of Tetrabutylphonium Hydroxide?
Tetrabutylphonium Hydroxide has a wide range of uses and is used in various fields of chemical industry.
In the industry of organic synthesis, it is a phase transfer catalyst and plays a special role. The method of phase transfer catalysis can make the reaction proceed smoothly between different phases. Tetrabutylphonium hydroxide can transfer nucleophiles in the aqueous phase to the organic phase, meet with organic substrates and react, increase the reaction rate, expand the reaction path, and enable many difficult reactions to be realized. For example, in etherification reactions, alkylation reactions, etc., it relies on its help to make the reaction conditions mild and the yield increases.
In the electronics industry, it is also indispensable. It can be used as a photolithography developer. In the manufacturing of semiconductors, printed circuit boards and other processes, it can accurately develop, etch away unwanted photoresists, retain required graphics, and lay the foundation for the fine manufacturing of electronic components. Because of its good development effect on photoresists, it can obtain clear and fine graphics, so it is important for electronic manufacturing.
In the field of surfactants, tetrabutylammonium hydroxide has unique properties. It can adjust the surface tension and assist in the formation of a stable emulsion system during emulsion polymerization. It can make the oil phase and water phase that are incompatible with each other evenly disperse, and the prepared emulsion has high stability. It plays an important role in the preparation of coatings, adhesives and other products. < Br >
In addition, in analytical chemistry, it can be used as a titrant. Because of its moderate alkalinity, it can be used for accurate titration analysis of some acidic substances, helping to determine the content and purity of substances, etc., providing accurate data for chemical analysis.
What are the physical properties of Tetrabutylphonium Hydroxide?
Tetrabutylphonium Hydroxide is an organic compound with unique physical properties.
This compound is often colorless to yellowish transparent liquid at room temperature. It looks like clear water, free of particulate impurities, and in a pure state. And its fluidity is quite good, pouring like a flow, without stagnation.
Its melting point is about -20 ° C, just like the cold of winter, and it can still maintain liquid agility at low temperatures. The boiling point is about 100 ° C. It boils when heated, and water vapor evaporates, showing the characteristics of matter changing with temperature.
Tetrabutylammonium hydroxide is very soluble in water, just like fish entering a river, instantly melting, and dissolving with water to form a uniform and stable solution. At the same time, it can also dissolve well in alcohols, such as ethanol, methanol, etc., which can be closely combined with it to form a homogeneous system.
Furthermore, its density is about 1.02 g/cm ³, which is similar to the density of water. When placed in water, it can sink or float, which is almost indistinguishable.
It has strong alkalinity, just like the heat of fire. When exposed to acid, it reacts violently, neutralizing acid and base, releasing energy. And its alkalinity often plays a key role in organic synthesis reactions, promoting the progress of many reactions. When storing, special attention should be paid. Due to its lively nature, it should be placed in a cool, dry and well-ventilated place, away from fire sources and oxidants, to prevent unexpected changes.
Tetrabutylphonium Hydroxide
Tetrabutylammonium hydroxide is an organic compound. It is active and has the characteristics of an alkali. At room temperature, it often exists in the form of an aqueous solution, showing a colorless to slightly yellow transparent liquid with a specific odor.
Tetrabutylammonium hydroxide has strong alkalinity, which is comparable to the inorganic strong base phase, and is widely used in the field of organic synthesis. First, it can be used as a phase transfer catalyst. The caustic molecule contains a large tetrabutylammonium cation, which can effectively promote the transfer of reactants between two phases that are incompatible with each other, accelerate the reaction process, and make the reaction more likely to occur. Second, in organic synthesis, it is often used as a base reagent. It can initiate many reactions such as dehalogenation of hydrogen and nucleophilic substitution.
However, this substance also poses certain risks. It is corrosive and can cause burns if it accidentally touches the skin or eyes. It is also irritating to the respiratory tract, inhaling its volatile aerosol, or damaging the respiratory system. When using, be sure to strictly follow safety procedures, such as protective clothing, protective glasses and gloves.
In terms of storage, it should be placed in a cool and ventilated place, away from fire and heat sources, to avoid decomposition or danger. Although it contributes a lot to organic synthesis, due to its special properties, it needs to be used and stored with extreme caution to ensure safety and effectiveness.
What should be paid attention to when storing and transporting Tetrabutylphonium Hydroxide?
Tetrabutylammonium hydroxide is a strong alkali. When storing and transporting, many points need to be paid attention to.
When storing, choose the first heavy container. When using corrosion-resistant containers, because tetrabutylammonium hydroxide has strong alkalinity, ordinary materials are prone to corrosion and leakage. For example, glass containers, some glass contains ingredients that can react with alkali, long-term contact or erosion of the glass, so special alkali-resistant glass or plastic containers should be selected. Like polyethylene and polypropylene materials, such plastics have good resistance to strong alkalis.
Temperature and humidity are also critical. Store in a cool, dry place away from direct sunlight. High temperature will cause its volatilization to accelerate, the concentration will change, and the temperature is too high or cause chemical reactions such as decomposition; in a high humidity environment, tetrabutylammonium hydroxide is easy to absorb moisture, which not only affects the accuracy of concentration, but also may cause its chemical properties to change due to excessive moisture. Generally, it is recommended that the storage temperature be between 5 ° C and 30 ° C.
The storage period cannot be ignored. It needs to be used according to the shelf life of the product description. Overdue or self-decomposition, reaction with environmental trace ingredients, etc., will cause quality degradation and affect the use effect.
During transportation, the packaging must be stable. Make sure that the container is well sealed to prevent leakage due to bumps and collisions. If it is for long-distance transportation, it is necessary to strengthen the packaging protection, such as wrapping with buffer material, and the transportation vehicle should maintain suitable temperature and humidity conditions.
At the same time, the transportation personnel need to be familiar with the dangerous characteristics of tetrabutylammonium hydroxide. In the event of leakage and other accidents, they can quickly deal with it according to the plan to ensure the safety of personnel and the environment is not polluted. In this way, the safety and quality of tetrabutylammonium hydroxide during storage and transportation can be guaranteed.
What are the common production methods of Tetrabutylphonium Hydroxide?
There are three common methods for preparing tetrabutylammonium hydroxide. The first is the ion exchange resin method. Take a solution of tetrabutylammonium bromide and make it flow through a strong basic anion exchange resin. The principle of ion exchange is that the hydroxide ion on the resin is exchanged with the bromine ion in the tetrabutylammonium bromide, resulting in the solution of tetrabutylammonium hydroxide. The beauty of this method is that the product is pure and the operation is relatively simple, but the regeneration of the ion exchange resin is quite complicated and the cost is relatively high.
The second is the metathesis reaction method. Tetrabutylammonium bromide and silver hydroxide are used as raw materials, and the two are combined to undergo a metathesis reaction. Bromine ions combine with silver ions to form silver bromide precipitation, leaving tetrabutylammonium hydroxide in the solution. The key to this reaction lies in the insolubility of silver bromide, which prompts the reaction to proceed to the right. However, silver hydroxide is unstable and easy to decompose. Careful preparation and storage are required, and the separation of silver bromide precipitation also requires fine operation.
The third is electrolysis. Using an aqueous solution of tetrabutylammonium bromide as an electrolyte, electrolysis is performed in a specific electrolysis device. Bromine ions lose electrons at the anode to form bromine elementals, and water at the cathode gives electrons to form hydrogen and hydroxide ions. Hydroxide ions combine with tetrabutylammonium ions to obtain tetrabutylammonium hydroxide. The advantage of this method is that the raw materials are relatively easy to obtain and can be produced continuously. However, the electrolysis process consumes a lot of energy and requires high equipment. It is necessary to properly control the electrolysis conditions in order to ensure the quality and output of the product.