Shanxian Chemical
Products

Tributylphosphine Oxide

Shanxian Chemical

Specifications

HS Code

398037

Packing & Storage
Packing 1 kg of Tributylphosphine Oxide packaged in a sealed, corrosion - resistant container.
Storage Tributylphosphine Oxide should be stored in a cool, dry, well - ventilated area. Keep it away from heat sources, flames, and oxidizing agents. Store in a tightly - sealed container to prevent moisture absorption and leakage. Avoid storage near incompatible substances to prevent potential chemical reactions. Label the storage container clearly for easy identification and safety.
Shipping Tributylphosphine Oxide is shipped in well - sealed, corrosion - resistant containers. It adheres to strict hazardous materials regulations, ensuring proper handling, labeling, and transportation to prevent spills and ensure safety during transit.
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General Information
Frequently Asked Questions
What are the main uses of Tributylphosphine Oxide?
Tributylphosphine oxide (Tributylphosphine Oxide) has a wide range of uses and is used in various fields of chemical industry.
First, it has a significant effect in the field of extraction and separation. Because of its excellent complexation ability to many metal ions, it is often used in the extraction of rare metals and precious metals. For example, in the separation and purification of rare earth elements, tributylphosphine oxide can achieve efficient separation by virtue of the difference in complexation stability with different rare earth ions. It can form a stable complex with metal ions, and this complex has good solubility in the organic phase, whereby metal ions can be extracted from the aqueous phase to the organic phase, and then re-extracted by suitable methods to achieve the enrichment and purification of metal ions.
Second, in the field of organic synthesis, it is also an important reagent. In many organic reactions, it can act as a ligand. In transition metal catalytic reactions, tributylphosphine oxide ligands can adjust the electronic properties and spatial structure of metal catalysts, which in turn affects the activity and selectivity of the reaction. For example, in some coupling reactions, the addition of this ligand can promote the reaction to proceed more efficiently and improve the yield of the target product. At the same time, in some specific organic synthesis routes, tributylphosphine oxide can also participate in the reaction, as a reactant to form new chemical bonds, helping to synthesize complex organic compounds.
Third, in the field of materials, it also contributes. In the preparation of polymer materials, it can be used as an additive. It can improve some properties of polymer materials, such as thermal stability and flame retardancy. Phosphorus in tributylphosphine oxide molecules has flame retardant properties. When added to polymer materials, a carbon layer with heat insulation and oxygen barrier can be formed when heated, thereby improving the flame retardancy of the material. And it has certain compatibility with polymer materials and will not cause serious negative effects on other properties of the material, so it is widely used in the modification of plastics, rubber and other polymer materials.
What are the Physical Properties of Tributylphosphine Oxide?
Tributylphosphine oxide is one of the organic phosphorus compounds. Its physical properties are quite different.
Looking at its properties, it is a white crystalline solid under normal conditions, with a pure appearance and a delicate state. Its melting point is in a specific range, about 150-154 ° C. This property is quite useful in the identification and separation of substances. Because the melting point is relatively fixed, it can be distinguished from other substances.
Furthermore, this substance has a certain solubility. In organic solvents, such as common toluene, chloroform, etc., it has considerable solubility. However, in water, its solubility is weak. This difference is due to its molecular structure characteristics. The carbon chain part of the molecule is a hydrophobic group, while the phosphine oxide part has a certain polarity, but it is not enough to dissolve it in large quantities in water.
The boiling point of tributylphosphine oxide cannot be ignored, which is about 370 ° C. The higher boiling point shows that the intermolecular force is strong, and it is not easy to vaporize and volatilize at ordinary temperatures. This property can maintain the stability of its material form in high-temperature chemical reaction environments, and does not easily escape, ensuring the integrity of the reaction system.
In addition, its density is also an important physical property, about 1.024g/cm ³. According to this, it can be used in specific experiments or industrial applications to accurately consider its dosage and occupied space, which is of great significance for controlling the reaction process. And this material is relatively stable at room temperature and pressure, and when it encounters hot topics, open flames or strong oxidizing agents, it is also potentially dangerous. Therefore, when using storage, it is necessary to pay careful attention to the surrounding environmental conditions.
Is Tributylphosphine Oxide Chemically Stable?
The properties of tributylphosphine oxide are still stable. Under normal conditions, it can withstand ordinary temperature and humidity, and chemical changes are not easy to occur.
Investigate its structure, the phosphorus-oxygen double bond is firm, so that its chemical properties tend to be stable. This structural feature allows it to maintain its inherent state in many reaction systems, and it is not easy to change violently with surrounding substances.
Looking at its physical properties, it is often a white crystal with a clear melting point, about 150 to 154 degrees Celsius. This property also helps its stability, because it is stable in the common temperature range, and it is not easy to volatilize or melt to change its properties.
In organic solvents, tributylphosphine oxide also has a certain solubility. However, this dissolution process is mostly physical dispersion, and no change in its chemical structure is caused, which also proves that its stability is good.
And in the air, although it is in contact with oxygen, the surface oxidation is extremely slow, and there is no appearance of rapid qualitative change. In conventional chemical operation scenarios, such as stirring, mixing, etc., it is also difficult to deteriorate due to ordinary mechanical action or slight thermal change in the outside world.
Although its performance is stable, it can still react under extreme conditions such as strong oxidizing agents or high temperatures, and the structure is broken. But in general, the chemical properties of tributylphosphine oxide are indeed stable in normal chemical work and storage environments.
In which industries is Tributylphosphine Oxide widely used?
Tributylphosphine oxide (Tributylphosphine Oxide) is widely used in many industries. In the industry of material synthesis, it often acts as a catalyst, which can effectively promote the efficient progress of the reaction. For example, in the preparation of polymer materials, it can speed up the polymerization reaction rate, make the polymer molecular structure more regular, thereby improving material properties, such as enhancing the strength and toughness of plastics, and making plastic products more durable.
In the field of chemical production, it is also an indispensable auxiliary. In specific organic synthesis reactions, it can precisely adjust the reaction path, improve the selectivity of the target product, reduce the occurrence of side reactions, and then improve product purity and reduce production costs. And in the extraction and separation process, with its unique chemical properties, it can efficiently separate and enrich specific metal ions, such as in the extraction of rare metals, helping to obtain high-purity rare metals from complex ore raw materials.
In the electronics industry, tributylphosphine oxide is also useful. In the manufacture of electronic materials, it can improve the electrical properties of materials, such as in the preparation of semiconductor materials, it can optimize the semiconductor crystal structure, improve the electron mobility, make electronic devices run more stably and efficiently, and help improve the performance of electronic products, such as faster computing speed of computer chips and better mobile phone signal processing.
In the pharmaceutical industry, it can be used as a key reagent in the drug synthesis process. Assisting in the construction of complex drug molecular structures, ensuring drug activity and stability is of great significance to the development and production of new drugs, promoting continuous progress in the field of medicine, and providing more effective drugs for human health. In short, tributylphosphine oxide plays a key role in many industries and has a profound impact on the development of various industries.
What is the production method of Tributylphosphine Oxide?
The method of preparing tributylphosphine oxide is obtained by reacting tributylphosphine with an oxidizing agent. Hydrogen peroxide is often used as an oxidizing agent, and the reaction is as follows: tributylphosphine meets hydrogen peroxide, and the two combine to produce tributylphosphine oxide and water. This reaction is quite convenient, and hydrogen peroxide is cheap and easy to purchase, so it is widely used.
When reacting, the temperature and reaction time need to be controlled. If the temperature is too high, it may cause the reaction to speed up, generate too much heat, and risk losing control; if the temperature is too low, the reaction will be slow and take a long time. Generally speaking, the temperature should be maintained in a moderate range, about room temperature to 50 degrees Celsius.
The reaction time is also critical. According to the reaction process, the progress of the reaction should be monitored by analytical means, such as thin layer chromatography or gas chromatography. When the reaction is complete, a mixture containing tributylphosphine oxide can be obtained.
After that, the steps of separation and purification must be carried out. The common method is distillation, which uses the difference between the boiling points of tributylphosphine oxide and other impurities to achieve the purpose of separation. Recrystallization can also be used to select a suitable solvent to crystallize and precipitate tributylphosphine oxide from the solution to obtain a pure product.
Another method of preparing tributylphosphine oxide using oxygen as an oxidant. In this process, tributylphosphine reacts with oxygen under specific conditions to form the target product. However, this method requires strict reaction conditions, and specific catalysts and reaction environments are required to make the reaction proceed smoothly. In contrast, the hydrogen peroxide method is simpler and more feasible, and is more commonly used in industrial production and laboratory preparation.